Bis[μ-4-methyl-2-(2-pyridyl­methyl­sulfan­yl)pyrimidine-κN 1]bis­[(trifluoro­methanesulfonato-κO)silver(I)]

نویسندگان

  • Huan-Huan Wang
  • Chao-Yan Zhang
  • Yue Cui
  • Qian Gao
  • Ya-Bo Xie
چکیده

In the centrosymmetric dinuclear title complex, [Ag(2)(CF(3)SO(3))(2)(C(11)H(11)N(3)S)(2)], the Ag(I) atom is coordinated by two N atoms from two 4-methyl-2-(2-pyridyl-methyl-sulfan-yl)pyrimidine ligands and one O atom from a trifluoro-methane-sulfonate anion in a distorted T-type coordination geometry. The ligand adopts a bidentate bridging coordination mode through one pyridyl N atom and one pyrimidine N atom. In the crystal structure, π-π inter-actions are present between adjacent pyrimidine rings, with a centroid-to-centroid distance of 3.875 (7) Å.

برای دانلود رایگان متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Bis(μ-nitrito-κ2 O:O)bis­[bis­(1-methyl-1H-imidazole-κN 3)(nitrito-κO)copper(II)]

In the binuclear title compound, [Cu(2)(NO(2))(4)(C(4)H(6)N(2))(4)], centro-symmetric-ally related complex mol-ecules are linked via weak Cu-O inter-actions, forming dimeric units. The Cu(II) atom displays an elongated square-pyramidal CuN(2)O(3) coordination geometry with a slight tetra-hedral distortion of the basal plane [maximum deviation = 0.249 (2) Å]. The dihedral angle formed by the imi...

متن کامل

(μ-Acetato-κ2 O:O′)[μ-2,6-bis­({bis­[(pyri­din-2-yl-κN)meth­yl]amino-κN}meth­yl)-4-methyl­phenolato-κ2 O:O](metha­nol-κO)dizinc bis­(perchlorate)

The binuclear title complex, [Zn2(C33H33N6O)(CH3COO2)(CH3OH)](ClO4)2, was synthesized by the reaction between 2,6-bis-({[bis-(pyridin-2-yl)meth-yl]amino}-meth-yl)-4-methyl-phenol (H-BPMP), Zn(OAc)2 and NaClO4. The two Zn(II) ions are bridged by the phenolate O atom of the octadentate ligand and the acetate group. An additional methanol ligand is terminally coordinated to one of the Zn(II) ions,...

متن کامل

Bis(nitrato-κO)bis­[4,4,5,5-tetra­methyl-2-(5-methyl-1H-imidazol-4-yl-κN 3)-2-imidazoline-1-oxyl 3-oxide-κO]nickel(II)

In the centrosymmetric mononuclear title complex, [Ni(NO(3))(2)(C(11)H(17)N(4)O(2))(2)], the Ni(II) atom displays a distorted octa-hedral coordination geometry and is six-coordinated by two N,O-bidentate nitronyl nitroxide radical ligands and two monodentate nitrate anions.

متن کامل

Bis[μ-1-(3,5-di­chloro­pyridin-2-yl)-2-(pyridin-3-yl­methyl­idene)hydrazine]bis­[(nitrato-κO)silver(I)] aceto­nitrile disolvate

In the centrosymmetric binuclear title complex, [Ag2(NO3)2(C11H8Cl2N4)2]·2CH3CN, the Ag(I) atom is four-coordinated and exhibits a highly distorted tetrahedral coordination sphere defined by three N atoms from two 1-(3,5-di-chloro-pyridin-2-yl)-2-(pyridin-3-yl-methyl-idene)hy-drazine ligands and one O atom from a nitrate anion. Inter-molecular N-H⋯O hydrogen bonds link the complex mol-ecules, r...

متن کامل

The cocrystal μ-oxalato-κ4 O 1,O 2:O 1′,O 2′-bis­(aqua­(nitrato-κO){[1-(2-pyridyl-κN)eth­ylidene]hydrazine-κN}copper(II)) μ-oxalato-κ4 O 1,O 2:O 1′,O 2′-bis­((methanol-κO)(nitrato-κO){[1-(2-pyridyl-κN)eth­ylidene]hydrazine-κN}copper(II)) (1/1)

The title cocrystal, [Cu(2)(C(2)O(4))(NO(3))(2)(C(7)H(9)N(3))(2)(H(2)O)(2)][Cu(2)(C(2)O(4))(NO(3))(2)(C(7)H(9)N(3))(2)(CH(4)O)(2)], is a 1:1 cocrystal of two centrosymmetric Cu(II) complexes with oxalate dianions and Schiff base ligands. In each mol-ecule, the Cu(II) centre is in a distorted octa-hedral cis-CuN(2)O(4) environment, the donor atoms of the N,N'-bidentate Schiff base ligand and the...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

عنوان ژورنال:

دوره 66  شماره 

صفحات  -

تاریخ انتشار 2010